Abstract
In this report, a simple template-free hydrothermal method was used to synthesise flower-like Ni(OH)2 structures modified with Ag and Cu. The Ni(OH)2 microflowers were formed via the self-assembly of ultrathin nanosheets with a thickness of approximately 2–3 nm. The incorporation of Ag and Cu at appropriate concentrations preserved the three-dimensional flower-like architecture of Ni(OH)2. For the Ag-Ni(OH)2 composite, Ag nanoparticles were uniformly dispersed on the Ni(OH)2 nanosheets. In contrast, no Cu(OH)2 phase was detected in the Cu-Ni(OH)2 composite, likely because of Cu substituting the Ni sites within the Ni(OH)2 lattice. Owing to their unique three-dimensional (3D) flower-like structure, large specific surface area, and enhanced physicochemical properties introduced by metal modification, these materials are potentially suitable for applications in electrochemical sensing, catalysis, and biomedical fields.
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