Synthesis and characterization of ZnxMn(1–x)Fe2O4
Tập 134 Số 1B (2025), Nghiên cứu
Tập 134 Số 1B (2025)

Synthesis and characterization of ZnxMn(1–x)Fe2O4

Nghiên cứu
https://doi.org/10.26459/hueunijns.v134i1B.7682
Đã xuất bản 2025-06-16
My Linh Nguyen Le
University of Education, Hue University, 34 Le Loi St., Hue City, Vietnam
Mai Nguyen Do
University of Sciences, Hue University, 77 Nguyen Hue St., Hue City, Vietnam

Tóm tắt

ZnxMn(1–x)Fe2O4 nanoparticles were successfully prepared in the isopropanol solvent with the hydrothermal method and the hydrothermal method combined with impregnation. The characterization of the samples by using X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier Transform Infrared (FTIR), and surface area analysis (BET) was conducted. The samples synthesized with the hydrothermal method had a phase composition of franklinite (Zn,Mn,Fe)(Fe,Mn)2O4. Meanwhile, the samples synthesized with the hydrothermal method combined with impregnation had the main phase composition of ZnxMn(1–x)Fe2O4. The Zn0.8Mn0.2Fe2O4 (ZnFe2O4/MnSO4 molar ratio = 4:1) sample exhibited the highest degree of structural order, with a BET surface area of 25.7 m2/g.

https://doi.org/10.26459/hueunijns.v134i1B.7682
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